SI Analytics Automatic Titrator TitroLine® 7500 KF trace for coulometric water determination

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Automatic Titrator for coulometric KF-Titration

The TitroLine® 7500 KF Trace is a compact, easy-to-use coulometric titrator for water determination according to Karl Fischer (KF) with a typical operating range of 1 ppm – 5% water.

The water determination according to Karl Fisher (KF) is the most selective and precise method for water determination. There is the volumetric and coulometric method. With the volumetric method the iodine is added accurately though a piston burette. The coulometric method generates the iodine directly in the titration vessel which allows the determination of very low water concentrations. The advantage is also that you do not have to determine the concentration of the titrant.

Suitable for chemical, petrochemical and pharmaceutical and other industries. For direct titration in the glass titration vessel the samples must be liquid or gaseous. The water from solid or high viscosity samples needs to be dissolved or extracted externally before or be evaporated by a head space oven TO 7280 or oven + autosampler TO 7280/TW 7650.

The TL 7500 KF trace has an exceptional high visibility full color graphic display which allows viewing even at extreme angles. The titration curve, but also other information such as the temperature of a connected headspace oven are clearly displayed on the display.

The three USB, two RS 232 and Ethernet interfaces makes the TL 7500 KF trace highly communicative. Various USB devices such as printers, barcode readers, keyboards can be connected. Analytical balances, PC and other SI Analytics devices such as the TO 7280 headspace oven can be connected via the RS-232 interfaces. The Ethernet interface allows data to be stored on a directly connected USB stick in PDF and CSV format as well as on shared network directories.

The parameters can be customized in each of the up to 50 methods. Through the user/password management, each user can be assigned individual rights. If you need even more methods or want to manage the data on a PC, you can use the TitriSoft PC software to control the TL 7500 KF trace. The TitriSoft 3.5P (TZ 3572) complies fully with 21 CFR, Part 11.

Key Features

  • Coulometric KF titration with automatic drift determination and correction
  • Standard methods for various applications such as water in%, water in ppm, water with KF oven, etc.
  • Statistical functions including average value and relative standard deviation
  • Configurable output: Short, Standard with curve, GLP
  • Formula editor for individual calculations
  • Output of results in ppm,%, mg, μg, mg / l. Unit individually adjustable
  • Also suitable for the determination of bromine number
  • The addition of the anolyte and the extraction of the titrated sample are carried out by the accessory Titration Stand (TM 235 KF) at the push of a button (only module 2 and 4)

Basic unit includes:

Basic unit, connection cable for generator electrode, connection cable for TM 235, TM 235 KF or TM 235 TO, USB keyboard TZ 3835, retaining clamp TZ 1749 for titration vessel, stand rod TZ 1748 and power supply 100-240 V.


SKU inclusions:

Module 1: 285220860

Basic unit, generator electrode TZ 1752 without junction + connection cable, magnetic stirrer TM 235, stand rod, titration vessel TZ 1751, micro double platinum electrode KF 1150.

TL 7500KF TRACE Module 2: 285220870

Basic unit, generator electrode TZ 1752 without junction + connection cable, TM 235 KF titration stand with integrated stirrer and pump, stand rod, titration vessel TZ 1754, micro double platinum electrode KF 1150.

TL 7500KF TRACE Module 3: 285220880

Basic unit, generator electrode TZ 1753 with junction + connection cable, magnetic stirrer TM 235, stand rod, titration vessel TZ 1751, micro double platinum electrode KF 1150.

TL 7500KF TRACE Module 4: 285220890

Basic unit, generator electrode TZ 1753 with junction + connection cable, TM 235 KF titration stand with integrated stirrer and pump, stand rod, titration vessel TZ 1754, micro double platinum electrode KF 1150.

TL 7500KF TRACE Module 5:

Basic unit, generator electrode TZ 1752 without junction + connection cable, magnetic stirrer TM 235, stand rod, titration vessel TZ 1754, micro double platinum electrode KF 1150. For use with manual KF oven TZ 1052 (not TO 7280!)

TL 7500KF TRACE Module 6:

Basic unit, generator electrode TZ 1752 with junction + connection cable, TM 235 TO titration stand with integrated stirrer, pump and valve, gas flow meter, 100 vials, grimper, bottle holder, stand rod, titration vessel TZ 1754, micro double platinum electrode KF 1150.

 TL 7500KF TRACE Module 6 TitriSoft Pharma:

Basic unit, generator electrode TZ 1752 with junction + connection cable, TM 235 TO titration stand with integrated stirrer, pump and valve, gas flow meter, 100 vials, grimper, bottle holder, stand rod, titration vessel TZ 1754, micro double platinum electrode KF 1150 and TitriSoft 3.5 P.

Specifications:

Measuring input indicator electrode Connector for double platium electrode with 2 × 4 mm sockets
Measuring input generator electrode Sockets: 2 × 4 mm, coded in color
Interfaces: 3 × USB (2 x USB-A and 1 × USB-B), 2 × RS-232-C and 1 x LAN
Display 3.5 inches – 1/4 VGA TFT graphic color display with 320 x 240 pixels
Housing material Polypropylene
Dimensions 15,3 x 18 x 29,6 cm (W x H x D)
Front keyboard Polyester coated
Weight 2,3 kg for basic device without magnetic stirrer TM 235 or TM 235 KF
Ambient conditions Ambient temperature: + 10 … + 40 °C for operation and storage Humidity according to EN 61 010, Part 1: max. relative humidity 80 % for temperatures up to 31 °C, linear decrease down to 50 % relative humidity at a temperature of 40 °C
Power supply: 100-240 V; 50/60 Hz, power input: 30 VA
CE-sign: EMC compatibility according to the Council Directive: 2004/108/EG; applied harmonized standards: EN 61326-1:2006
Low-voltage directive according to the Council Directive 2006/95/EG Testing basis EN 61 010, Part 1
Magnetic stirrer TM 235 with Power supply TZ 1855, for vessels up to 500 ml, agitator speed infinitely adjustable from 500 – 2000 r/min, for the connection to TitroLine® 7XXX and TITRONIC® 500

 

Titration stand TM235 KF

Pump Free volume flow- air-: flow rate 2.25 l / min
Delivery pressure max. 1.5 bar.
Flow rate liquid medium ca. 0.8 l / min
Stirring speed 50 to 1000 U/min
Hoses PVC- hose (outer diameter 6 x 1 mm)
PTFE- hose (outer diameter 4 x 0.5 mm)
Dimensions 80 x 130 x 250 mm, (W x H x D (height without stand rod)
Weight 1kg

Description

Automatic Titrator for coulometric KF-Titration

The TitroLine® 7500 KF Trace is a compact, easy-to-use coulometric titrator for water determination according to Karl Fischer (KF) with a typical operating range of 1 ppm – 5% water.

The water determination according to Karl Fisher (KF) is the most selective and precise method for water determination. There is the volumetric and coulometric method. With the volumetric method the iodine is added accurately though a piston burette. The coulometric method generates the iodine directly in the titration vessel which allows the determination of very low water concentrations. The advantage is also that you do not have to determine the concentration of the titrant.

Suitable for chemical, petrochemical and pharmaceutical and other industries. For direct titration in the glass titration vessel the samples must be liquid or gaseous. The water from solid or high viscosity samples needs to be dissolved or extracted externally before or be evaporated by a head space oven TO 7280 or oven + autosampler TO 7280/TW 7650.

The TL 7500 KF trace has an exceptional high visibility full color graphic display which allows viewing even at extreme angles. The titration curve, but also other information such as the temperature of a connected headspace oven are clearly displayed on the display.

The three USB, two RS 232 and Ethernet interfaces makes the TL 7500 KF trace highly communicative. Various USB devices such as printers, barcode readers, keyboards can be connected. Analytical balances, PC and other SI Analytics devices such as the TO 7280 headspace oven can be connected via the RS-232 interfaces. The Ethernet interface allows data to be stored on a directly connected USB stick in PDF and CSV format as well as on shared network directories.

The parameters can be customized in each of the up to 50 methods. Through the user/password management, each user can be assigned individual rights. If you need even more methods or want to manage the data on a PC, you can use the TitriSoft PC software to control the TL 7500 KF trace. The TitriSoft 3.5P (TZ 3572) complies fully with 21 CFR, Part 11.